Practical Synthesis of 3β-Amino-5-cholestene and Related 3β-Halides Involving i-Steroid and Retro-i-Steroid Rearrangements

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Practical Synthesis of 3 -Amino-5-cholestene and Related 3 -Halides Involving i-Steroid and Retro-i-Steroid Rearrangements

Derivatives of 3 -amino-5-cholestene (3 -cholesterylamine) are of substantial interest as cellular probes and have potential medicinal applications. However, existing syntheses of 3 -amino-5-cholestene are of limited preparative utility. We report here a practical method for the stereoselective preparation of 3 -amino-5-cholestene, 3 -chloro-5-cholestene, 3 -bromo-5-cholestene, and 3 -iodo-5-ch...

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ژورنال

عنوان ژورنال: Organic Letters

سال: 2008

ISSN: 1523-7060,1523-7052

DOI: 10.1021/ol802343z